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As an example, Eu(TMHD)3 and sodium were placed in two crucibles inside the furnace, and hydrogen gas was introduced to the chamber, as well. Hydrogen entrained the saturated vapors of Eu(TMHD)3 and sodium. This gas mixture was then ignited when it entered the flame. The starting materials decomposed in the flame forming corresponding oxides and further formed silica glass nanoparticles that contained europium. As another example, an ethanol solution containing Eu(NO3)3 and Y(NO3)3 was sprayed and introduced to the chamber from the bottom inlet. Hydrogen gas was also introduced to the chamber from the same inlet. The droplets were ignited once they entered the diffusion flame. Strobel et al. [47], invented a process for the production of nanoparticles comprising a non-segregated submicron mixture of individual nanoparticles by flame spray pyrolysis. In this method, two spray nozzles are connected to two precursor reservoirs at an angle Fig. (9). The reservoirs are filled with two different precursors. The precursors are sprayed and ignited to produce two spray flames oriented at an angle with respect to each other. Depending on the distance and angle between the nozzles, some portion of the two flames may overlap or at least the vapors of the two precursors will mix to produce multicomponent particles.

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الكلية كلية هندسة المواد     القسم قسم هندسة السيراميك ومواد البناء     المرحلة 7
أستاذ المادة شاكر جاهل ادريس المحنا       10/01/2018 17:49:24
formation in aqueous solution droplets of sodium chloride, ammonium sulphate, and suspensions of silicon dioxide in water. In their study, partly dried droplets were caught in an oil bath and were characterized by an optical microscope. They observed several single cubic crystals of sodium chloride on the edge of the caught droplet.
On the other hand, an amorphous crust formed on the ammonium sulphate droplet and the droplet containing silica sols lead to the formation of a similar crust. Their findings about the cubic morphology of sodium chloride particles are consistent with other studies [5, 6, 10]. Zhou et al. [11],
investigated the effect of the solvent on the morphology of spray dried polymethyl methacrylate (PMMA) particles. They found that the product PMMA particles derived from the PMMA-acetone dilute solution had a smaller particle size than those from PMMA-tetrahydrouran dilute solution. They
attributed this to the better solubility of PMMA in acetone than in tetrahydrouran. They observed that, using various solvents, several particle morphologies including solid, porous, and honeycomb spheres can be obtained. Lin and Gentry [12] investigated the effects of drying temperature, initial concentration and solubility of the solute, and the heat of solute crystallization on the morphology and shape of the particles produced from suspended solution droplets.


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